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HRID2166325

反应详情

EQUATION

反应方程式

HRID 2166325 的结构方程式

REACTANTS

反应物

2
反应SMILES：O=Cc1ccc([N+](=O)[O-])cc1
HCID541

4-Nitrobenzaldehyde

C7H5NO3

反应SMILES：Cc1ccc(C)nn1
HCID527031

3,6-dimethylpyridazine

C6H8N2

PRODUCTS

产物

1
反应SMILES：O=[N+]([O-])c1ccc(C=Cc2ccc(C=Cc3ccc([N+](=O)[O-])cc3)nn2)cc1
HCID54059565

未命名化合物

收率 44.4%

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CC(=O)OC(C)=O
溶剂HCID7918

Acetic anhydride

C4H6O3

PROCEDURE

实验过程

First, 24 g of 3,6-dimethylpyridazine and 60 g of p-nitrobenzaldehyde were dissolved in 1 liter of acetic anhydride, then heated under reflux so as to obtain 33 g of 3,6-di(p-nitrostyryl)pyridazine.

WORKUP

后处理

  1. temperatureheated
  2. temperatureunder reflux so as