HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzaldehyde → 3,6-Di(o-nitrostyryl)pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzaldehyde | HCID 11101 | — |
| Reactant | 3,6-Dimethylpyridazine | HCID 527031 | — |
| Solvent | Propionic anhydride | HCID 31263 | — |
| Product | 3,6-Di(o-nitrostyryl)pyridazine | HCID 54426522 | 39.8% |
Reaction Steps
First, 24 g of 3,6-dimethylpyridazine and 67 g of o-nitrobenzaldehyde were dissolved in 600 ml of propionic anhydride, then heated under reflux so as to obtain 33 g of 3,6-di(o-nitrostyryl)pyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04945021 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-c25a530e4c844891873c7980d191ca64 |
| Source note | uspto-grants-1990_07 |