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HRID2166326

反应详情

EQUATION

反应方程式

HRID 2166326 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccccc1[N+](=O)[O-]
HCID11101

2-Nitrobenzaldehyde

C7H5NO3

结构：Cc1ccc(C)nn1
HCID527031

3,6-dimethylpyridazine

C6H8N2

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccccc1C=Cc1ccc(C=Cc2ccccc2[N+](=O)[O-])nn1
HCID54426522

未命名化合物

收率 39.8%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(=O)OC(=O)CC
溶剂HCID31263

Propanoic anhydride

C6H10O3

PROCEDURE

实验过程

First, 24 g of 3,6-dimethylpyridazine and 67 g of o-nitrobenzaldehyde were dissolved in 600 ml of propionic anhydride, then heated under reflux so as to obtain 33 g of 3,6-di(o-nitrostyryl)pyridazine.

WORKUP

后处理

  1. temperatureheated
  2. temperatureunder reflux so as