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HRID2166327

反应详情

EQUATION

反应方程式

HRID 2166327 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(C)nn1
HCID527031

3,6-dimethylpyridazine

C6H8N2

结构：O=Cc1ccc([N+](=O)[O-])c(Cl)c1
HCID3769779

3-chloro-4-nitrobenzaldehyde

C7H4ClNO3

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(C=Cc2ccc(C=Cc3ccc([N+](=O)[O-])c(Cl)c3)nn2)cc1Cl
HCID54154328

未命名化合物

收率 18.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)OC(C)=O
溶剂HCID7918

Acetic anhydride

C4H6O3

PROCEDURE

实验过程

First, 28 g of 3,6-dimethylpyridazine and 98 g of 3-chloro-4-nitrobenzaldehyde were dissolved in 1.5 liters of acetic anhydride to produce 21 g of 3,6-di(3-chloro-4-nitrostyryl)-pyridazine.