HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,6-Dimethylpyridazine → 3,6-Di(3-chloro-4-nitrostyryl)-pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,6-Dimethylpyridazine | HCID 527031 | — |
| Reactant | 3-Chloro-4-nitrobenzaldehyde | HCID 3769779 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | 3,6-Di(3-chloro-4-nitrostyryl)-pyridazine | HCID 54154328 | 18.3% |
Reaction Steps
First, 28 g of 3,6-dimethylpyridazine and 98 g of 3-chloro-4-nitrobenzaldehyde were dissolved in 1.5 liters of acetic anhydride to produce 21 g of 3,6-di(3-chloro-4-nitrostyryl)-pyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04945021 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-3bff879890cb486a97be29289d454226 |
| Source note | uspto-grants-1990_07 |