HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2166338Generated: November 1, 2026
3-Chloro-2-methyl-1-propene → HCID 23039515, compound
https://huagongshe.com/reaction/2166338
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,5-Dichloro-3-hydroxypyridazine | HCID 73247 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23039515 | HCID 23039515 | 36.9% |
Reaction Steps
To 50 ml of N,N-dimethylformamide were suspended 10 g of 4,5-dichloro-3(2H)-pyridazinone, 27 g of 3-chloro-2-methylpropene and 8.4 g of potassium carbonate. The mixtured solution was stirred for 5 hours at 40° C. Then, the procedures in Preparation Example 2 were repeated to give 4.9 g of the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04945091 |
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| Source dataset | uspto-grants-1990_07 |
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| ORD ID | ord-112dcfeb10c242c68c5acaaeed4a5f8e |
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| Source note | uspto-grants-1990_07 |
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