HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylamine → HCID 86744120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | HCID 23039617 | HCID 23039617 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86744120 | HCID 86744120 | — |
Reaction Steps
1-Hexadecyloxy-3-[4-(methanesulfonyloxy)butoxy]-2-methylenepropane (from Preparation 7) (1.77 g) was refluxed with 33% trimethylamine in ethanol at 50° C. for 4 hours. Excess trimethylamine and ethanol were removed in vacuo. The product was recrystallized from chloroform/acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04945098 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-a28bc141679e45c4b4e92aa61250a136 |
| Source note | uspto-grants-1990_07 |