Aniline → HCID 13150870, compound

HRID 2166597Notes

Reaction equation

HRID 2166597 reaction equation
[O:1]1[CH:6]([C:7]([OH:9])=[O:8])[CH:2]1[C:3]([OH:5])=O.[C:10]1([K])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.C(Cl)(=O)C(Cl)=O.[NH2:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[C:24]1([NH:23][C:3](=[O:5])[CH:2]2[O:1][CH:6]2[C:7]([O:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[O:8])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1

Participants

4

Reactant 3

HCID 6115AnilineHCID 65578Oxalyl chlorideHCID 178524971HCID 178524971, compound

Product 1

HCID 13150870HCID 13150870, compoundYield 19.7%

Procedure

Following the procedure of Example 1, monophenyl potassium epoxysuccinate (3.64 g) was successively treated with oxalyl chloride (2.10 g) and aniline (1.4 g) to give 0.82 g of phenyl N-phenyl-2,3-epoxysuccinamate (Compound No. 28) as colorless needles melting at 121° C.

Sources & evidence

ORD record
ord-381dbc9fa2b3470e8c7f6fb4379888a3
Source dataset
uspto-grants-1983_06
Patent number
US04387238

Reaction notes

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