HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → allyl N-phenyl-2,3-epoxysuccinamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 178455845 | HCID 178455845 | — |
| Product | allyl N-phenyl-2,3-epoxysuccinamate | HCID 13150874 | 50.7% |
Reaction Steps
Following the procedure of Example 1, monoallyl potassium epoxysuccinate (2.1 g) was successively treated with oxalyl chloride (1.26 g) and aniline (1.86 g) to give 1.24 g of allyl N-phenyl-2,3-epoxysuccinamate (Compound No. 30) as colorless needles melting at 32° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04387238 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-e3b567c51b564631b0ab7bafbf747871 |
| Source note | uspto-grants-1983_06 |