HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylcyclohexylamine → HCID 13150840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylcyclohexylamine | HCID 7514 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 178461626 | HCID 178461626 | — |
| Product | HCID 13150840 | HCID 13150840 | 50.2% |
Reaction Steps
Following the procedure of Example 1, monoethyl potassium epoxysuccinate (1.0 g) was successively treated with oxalyl chloride (0.75 g) and N-methylcyclohexylamine (1.15 g) to give 0.64 g of ethyl N-methyl-N-cyclohexyl-2,3-epoxysuccinamate (Compound No. 31) as colorless needles melting at 52°-55° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04387238 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-46e7f64e9a674477ae115beb55b9c219 |
| Source note | uspto-grants-1983_06 |