HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine, hydrochloride → HCID 20499838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 178461626 | HCID 178461626 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20499838 | HCID 20499838 | 39.6% |
Reaction Steps
Following the procedure of Example 53, monoethyl potassium epoxysuccinate (1.0 g) was successively treated with oxalyl chloride (0.75 g) and a mixture of dimethylamine hydrochloride (1.23 g) and triethylamine (2.04 g) to give 0.37 g of ethyl N,N-dimethyl-2,3-epoxysuccinamate (Compound No. 85) as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04387238 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-bb325c0265f3493c8c8b19bc2f20972f |
| Source note | uspto-grants-1983_06 |