HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-(Bromomethyl)phenyl)methanol → 3-(Bromomethyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-(Bromomethyl)phenyl)methanol | HCID 19032333 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(Bromomethyl)benzaldehyde | HCID 7127825 | 55% |
Reaction Steps
3-Bromomethylbenzyl alcohol (1.015 g, 5 mmol) and activated manganese (IV) oxide (10 g) in acetone (30 ml) were stirred at 20° C. for 22 h. The reaction mixture was filtered and the filtrate evaporated in vacuo to yield 3-bromomethylbenzaldehyde as a pale yellow liquid (547 mg, 55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04389410 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-cfa0f2c3396a4999a7290f5651781467 |
| Source note | uspto-grants-1983_06 |