HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluorine → HCID 12886210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluorine | HCID 24524 | — |
| Reactant | HCID 8008517 | HCID 8008517 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 12886210 | HCID 12886210 | — |
Reaction Steps
In the same manner as in Example 1, methyl 3-(4-chlorophenyl)pyruvate is dissolved in acetonitrile (500 ml) and reacted with fluorine at -10° C. After the same work-up as in Example 1, the resulting crude product is rectified to give syrupy methyl 3-(4-chlorophenyl)-3-fluoropyruvate (7.49 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04390702 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-f289966e971c469487f778ca69f6a8b5 |
| Source note | uspto-grants-1983_06 |