HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluorine → HCID 20497530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluorine | HCID 24524 | — |
| Reactant | Methyl 3-(2-nitrophenyl)-2-oxopropanoate | HCID 3018840 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20497530 | HCID 20497530 | — |
Reaction Steps
In the same manner as in Example 1, methyl 3-(2-nitrophenyl)pyruvate (2.23 g; 10 mmol) is dissolved in acetonitrile (50 g) and reacted with fluorine. By distilling off the solvent under reduced pressure, there is obtained a crude product, whicch is rectified to give methyl 3-(2-nitrophenyl)-3-fluoropyruvate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04390702 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-5a24c407c90a4180b97a6c65afe37a54 |
| Source note | uspto-grants-1983_06 |