Carbon Disulfide → HCID 20497544, compound

Participants

Reaction Conditions

Reaction Steps

To 10 g of N-allylethylendiamine (0.1 moles) dissolved in 50 cc of ethanol there were admixed, under stirring, 7.6 g of CS2 (0.1 moles) dissolved in 50 cc ethanol, the temperature being maintained at about 5° C. Once the addition is accomplished, stirring is continued for another 15 minutes, after which the resulting precipitate is filtered and, after washing with ethanol, consists of 15.6 g of white crystals having a m.p. of 125° C. (with decomposition) of N-(2'-allylaminoethyl)dithiocarbamic acid having the following structure of an internal salt: ##STR20##

Provenance & Evidence