Benzoyl chloride → HCID 178486250, compound

HRID 21671Notes

Reaction equation

HRID 21671 reaction equation
[C:1]([NH:5][NH:6][PH:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1C)=[O:8])([CH3:4])([CH3:3])[CH3:2].[CH2:16](N(CC)CC)C.[C:23](Cl)(=[O:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>C(OCC)C.CCCCCC>[C:1]([N:5]([C:23](=[O:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[N:6]([PH:7]([C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1)=[O:8])[CH3:16])([CH3:2])([CH3:3])[CH3:4]

Participants

6

Reactant 3

HCID 7412Benzoyl chlorideHCID 8471TriethylamineHCID 178424407HCID 178424407, compound

Product 1

HCID 178486250HCID 178486250, compound

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 8058HexaneSolvent

Procedure

N'-t-butyl-N-(methylphenyl)phosphinylhydrazine (0.7 g) and triethylamine (3 ml) were stirred in diethyl ether (30 ml) at room temperature. Slowly, benzoyl chloride (1.2 g) was added dropwise to the reaction mixture. After stirring 1 hour at room temperature, the reaction mixture was diluted with hexane and the solid product filtered off. The white solid melted at 175°-178° C.

Workup

  1. filtrationthe solid product filtered off

Sources & evidence

ORD record
ord-b9c6965e732647468868ecc1d00fc302
Source dataset
uspto-grants-1995_06
Patent number
US05424333

Reaction notes

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