HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86674214, compound → HCID 71060109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86674214 | HCID 86674214 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 71060109 | HCID 71060109 | — |
Reaction Steps
A solution of methyl 2′-formyl-3′-(prop-1-en-2-yl)-5′-(trifluoromethyl)-[1,1′-biphenyl]-4-carboxylate (122 mg, 0.35 mmol) in MeOH (10 mL) was hydrogenated using H-Cube (10 Bar H2) at 40° C. at a flow rate of 1 mL/min. The resulting solution was concentrated to yield the title compound, which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045389B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-a7dd574d98224d69b6903de421ace3b5 |
| Source note | uspto-grants-2015_06 |