HRID2167201

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69415

Amyl isothiocyanate

C6H11NS

结构：CC(C)=CCC/C(C)=C/CC/C(C)=C/CC/C(C)=C/CO

HCID5281365

Geranylgeraniol

C20H34O

结构：CC(C)=CCC/C(C)=C/CC/C(C)=C/CC/C(C)=C/COC(=S)Nc1cccnc1

HCID86701128

未命名化合物

PRODUCTS

生成物

$结构：CCCCNC(=S)OC/C=C(\C)CC/C=C(\C)CC/C=C(\C)CCC=C(C)C$

HCID86701130

未命名化合物

收率 60%

PROCEDURE

实验过程

Similar to the preparation of 38a, the reaction of alcohol 1 with pentyl isothiocyanate afforded the desired compound 10e in 60% yield (135 mg) as a viscous oil. Column (EtOAc/Hexane); TLC Rf: 0.70 (10% EtOAc/hexanes); LCMS: MS (m/z): 406.1 (M+H).