HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromopropoxy)-4-fluorobenzene → HCID 11548210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromopropoxy)-4-fluorobenzene | HCID 260004 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11548210 | HCID 11548210 | 43.7% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0182 g, 0.0621 mmol) and 3-bromopropyl 4-fluorophenyl ether (0.0173 g, 0.0742 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0143 g, 43.7%). EI-MS m/z 446 (M+) Rt (1.96 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045469B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-44e37e17971348279fc15a1443571dbc |
| Source note | uspto-grants-2015_06 |