Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methylbenzamide | HCID 69274 | — |
| Reactant | (Chlorothio)formyl chloride | HCID 75990 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12437398 | HCID 12437398 | — |
Reaction Steps
To a toluene (60 mL) suspension of 4-methylbenzamide (20 g), chlorocarbonylsulfenyl chloride (15 mL) was added, and the resultant was stirred at 120° C. for 3 hours. The reaction solution was concentrated under reduced pressure. The obtained solid was washed with hexane to obtain the title compound (24 g) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09045466B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
|---|
| ORD ID | ord-5ed1af5e37e440bf846c1d5f99b4c804 |
|---|
| Source note | uspto-grants-2015_06 |
|---|
