HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,5-Dibromobarbituric acid → HCID 86720747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,5-Dibromobarbituric acid | HCID 94877 | — |
| Reactant | HCID 18525961 | HCID 18525961 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86720747 | HCID 86720747 | 71.7% |
Reaction Steps
To a tetrahydrofuran (5.0 mL) solution of 3-(acetyl)-6-tert-butylpyridin-2(1H)-one (0.50 g), 5,5-dibromobarbituric acid (0.41 g) was added, and the resultant was heated to reflux for 2 hours. A deposit formed during the course of concentration of the reaction solution under reduced pressure was filtered to obtain the title compound (0.28 g) as a light brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045466B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-1cc9fc32d2e34f9583424afce5384b1b |
| Source note | uspto-grants-2015_06 |