HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2168253Generated: October 30, 2026
HCID 86710212, compound → HCID 178510332, compound
https://huagongshe.com/reaction/2168253
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 86710212 | HCID 86710212 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178510332 | HCID 178510332 | — |
Reaction Steps
N-{1-[5-cyano-7-({[2-(trimethylsilyl)ethyl]oxy}methyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl]-4-piperidinyl}benzamide D44 (69 mg) and LiBF4 (85 mg, 0.9 mmol) were dissolved in MeCN (10 ml) and then the reaction mixture was heated at 80° C. for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09045485B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-19a9f86acbf341768efa6e7ea9e4095b |
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| Source note | uspto-grants-2015_06 |
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