HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178511244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178453599 | HCID 178453599 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178511244 | HCID 178511244 | — |
Reaction Steps
To a solution of tert-butyl(trans-4-cyanocyclohexyl)methylcarbamate (500 mg) in dichloromethane (10 mL) was slowly added trifluoroacetic acid (2 mL) at 0° C. The reaction mixture was warmed to room temperature, stirred for 1 hour and concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045420B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-6cf4e1ac54774cbfa9978d25dc48346e |
| Source note | uspto-grants-2015_06 |