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HRID2168434

反应详情

EQUATION

反应方程式

HRID 2168434 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OI1(OC(C)=O)(OC(C)=O)OC(=O)c2ccccc21
HCID159087

Triacetoxyperiodinane

C13H13IO8

结构：CC1(C)CCC(CO)=C(c2ccc(Cl)cc2)C1
HCID66713205

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)CCC(C=O)=C(c2ccc(Cl)cc2)C1
HCID87279414

2-(4-Chlorophenyl)-4,4-dimethyl-1-cyclohexene-1-carboxaldehyde

C15H17ClO

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

To a solution of EXAMPLE 494F in dichloromethane (120 mL) at 0° C. was added Dess-Martin periodinane (17.7 g) and the reaction was allowed to warm to room temperature.