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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2168434Generated: October 31, 2026

Triacetoxyperiodinane → 2-(4-Chlorophenyl)-4,4-dimethyl-1-cyclohexene-1-carboxaldehyde

https://huagongshe.com/reaction/2168434

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriacetoxyperiodinaneHCID 159087—
ReactantHCID 66713205HCID 66713205—
SolventDichloromethaneHCID 6344—
Product2-(4-Chlorophenyl)-4,4-dimethyl-1-cyclohexene-1-carboxaldehydeHCID 87279414—

Reaction Steps

To a solution of EXAMPLE 494F in dichloromethane (120 mL) at 0° C. was added Dess-Martin periodinane (17.7 g) and the reaction was allowed to warm to room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09045420B2
Source datasetuspto-grants-2015_06
ORD IDord-0ed3310abe1346fc98730674c5d593c9
Source noteuspto-grants-2015_06