HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178446422, compound → HCID 178446402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178446422 | HCID 178446422 | — |
| Reactant | HCID 178519962 | HCID 178519962 | — |
| Product | HCID 178446402 | HCID 178446402 | 94.8% |
Reaction Steps
This compound was prepared following the same method as described for 5-benzyloxy-6-hydroxy-2-(1-phenyl-cyclopentylmethyl)-pyrimidine-4-carboxylic acid cyclopropyl-(2-hydroxyethyl)-amide (285) from 5-benzyloxy-6-hydroxy-2-(1-phenyl-cyclopentylmethyl)-pyrimidine-4-carboxylic acid [2-(tert-butyl-dimethylsilanyloxy)-ethyl]-(2,2-dimethyl-propyl)-amide (300) (350 mg, 0.55 mmol). The product was obtained as a light yellow sticky solid (270 mg, 94.03%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045486B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-ea1df6086e1249c9ad8c8dd6a27d3c67 |
| Source note | uspto-grants-2015_06 |