Hippuric Acid → HCID 86595984, compound

HRID 2170014Notes

Reaction equation

HRID 2170014 reaction equation
C(=O)([O-])[O-].[Sr+2:5].[C:6]([OH:18])(=[O:17])[CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[O:10]>O>[C:6]([O-:18])(=[O:17])[CH2:7][NH:8][C:9]([C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)=[O:10].[Sr+2:5].[C:6]([O-:18])(=[O:17])[CH2:7][NH:8][C:9]([C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)=[O:10]

Participants

4

Procedure

Strontium carbonate (0.5 g, 3.39 mmol) and hippuric acid (1.215 g, 6.77 mmol) in water (30 ml) were stirred at 70.degree. C. for 5 hours. The mixture was filtered and the filtrate was evaporated to dryness and dried in vacuo at ambient temperature. Yield 1.25 g (83%).

Workup

  1. filtrationThe mixture was filtered
  2. customthe filtrate was evaporated to dryness
  3. customdried in vacuo at ambient temperature

Sources & evidence

ORD record
ord-ef3b40361d2e48609293c5e5fc22a044
Source dataset
uspto-grants-2015_06
Patent number
US09050312B2

Reaction notes

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