HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 90386794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | HCID 90386782 | HCID 90386782 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90386794 | HCID 90386794 | 98% |
Reaction Steps
A mixture of Example 4e (0.05 g, 0.088 mmol) and propan-1-amine (1 mL, 12.16 mmol) in methanol (0.5 mL) in a sealed tube was heated by microwave at 120° C. for 2 hours, cooled and concentrated to afford the title compound (0.05 g, 98%). The product was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09050346B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-b3a34460d6554e7f804a64cfd2db9d5b |
| Source note | uspto-grants-2015_06 |