HCID 90281393, compound → HCID 90281431, compound

Participants

Reaction Steps

To a mixture of Compound 41B (100 mg, 0.14 mmol) in 15 ml of ethanol, 0.05 ml of hydrazine monohydrate was added and the reaction mixture was stirred at room temperature for 10 min. The solvent was removed and the residue was purified by RP-HPLC eluting with acetonitrile/H2O (with 0.1% TFA) to afford the title product. MS (m/z) 592.20 [M+H]+.

Provenance & Evidence