HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 71075681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 63717133 | HCID 63717133 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71075681 | HCID 71075681 | — |
Reaction Steps
Benzoyl chloride (1.1 equiv) was added to a solution of N-(1-phenylpropyl)-1H-indole-5-carboxamide in CH2Cl2, Et3N (1.3 equiv) at room temperature. After the reaction was completed, the solvent was evaporated and the residual was purified by silica gel column chromatography to get the product. LC-MS 383 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051265B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-d07632d5b0d8436f880b4abe05866b48 |
| Source note | uspto-grants-2015_06 |