HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl methyl ether → HCID 67168854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | HCID 60047515 | HCID 60047515 | — |
| Product | HCID 67168854 | HCID 67168854 | 96% |
Reaction Steps
The title compound was prepared in 96% yield (355 mg, colorless syrup) from tert-butyl 4-(3-hydroxyphenoxy)piperidine-1-carboxylate (300 mg, 1.02 mmol) and 1-bromo-2-methoxyethane (171 mg, 1.23 mmol) at a reaction temperature of 60° C. by the similar manner in Step-1 of Intermediate-2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051296B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-a68b76c95bb94293852bc8c6e67de64c |
| Source note | uspto-grants-2015_06 |