HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethoxy)thiophenol → HCID 18538977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethoxy)thiophenol | HCID 2777360 | — |
| Reactant | 1-(tert-Butoxycarbonyl)-4-(methanesulfonyloxy)piperidine | HCID 4184869 | — |
| Product | HCID 18538977 | HCID 18538977 | 41% |
Reaction Steps
The title compound was prepared in 41% yield (0.66 g, colorless oil) from tert-butyl 4-((methylsulfonyl)oxy)piperidine-1-carboxylate (1.20 g, 4.30 mmol) and 4-(trifluoromethoxy)benzenethiol (1.00 g, 5.15 mmol) by the similar manner in Step-1 of Intermediate-4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051296B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-39abf1cf041f41b08cbf0b7839dcf6dc |
| Source note | uspto-grants-2015_06 |