HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Carboxybenzaldehyde → HCID 62925667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Carboxybenzaldehyde | HCID 12077 | — |
| Reactant | N-Methyl-o-phenylenediamine | HCID 78498 | — |
| Product | HCID 62925667 | HCID 62925667 | 51% |
Reaction Steps
The title compound was prepared in 51% yield (428 g, a slight brown solid) from 3-formylbenzoic acid (500 mg, 3.33 mmol) and N1-methylbenzene-1,2-diamine (407 mg, 3.33 mmol) by the similar manner in Intermediate-7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051296B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-64840ed48c61423492c755fb1ca6eb35 |
| Source note | uspto-grants-2015_06 |