HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54049649, compound → 3-Ethyl-4-formylbenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54049649 | HCID 54049649 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Ethyl-4-formylbenzonitrile | HCID 17819327 | — |
Reaction Steps
A solution of 1.3 g (8.27 mmol) of 4-formyl-3-vinylbenzonitrile in 35 ml of ethanol is mixed with 880 mg of 10% palladium on carbon and vigorously stirred under a hydrogen atmosphere for 2 h. The suspension is filtered through a layer of kieselguhr, the residue is washed with ethanol, and the filtrate is concentrated. The residue (890 mg) is employed without further purification in the following stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051316B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-6575eeae044e4e2dba095542d25e31e9 |
| Source note | uspto-grants-2015_06 |