HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 178526230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 4-Bromo-1H-pyrazolo[3,4-c]pyridine | HCID 46916247 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178526230 | HCID 178526230 | 69.5% |
Reaction Steps
mCPBA (270 mg) was added to a CHCl3 (5 ml) suspension containing 4-bromo-1H-pyrazolo[3,4-c]pyridine (197 mg), followed by stirring at room temperature for 10 minutes. IPE (10 ml) was added to the reaction solution and a solid precipitate was collected by filtration. A white solid of 4-bromo-1H-pyrazolo[3,4-c]pyridine 6-oxide (148 mg) was thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051310B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-88ff4c10f8a84eb1b8710dbc067a4285 |
| Source note | uspto-grants-2015_06 |