HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2171345Generated: October 31, 2026
Potassium Carbonate → HCID 135743575, compound
https://huagongshe.com/reaction/2171345
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86724161 | HCID 86724161 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 135743575 | HCID 135743575 | — |
Reaction Steps
To a mixture of N-(2-bromoethyl)-2,6-dichloropyrimidin-4-amine (10 g, 18 mmol) in 1,4-dioxane (30 mL) and water (30.0 mL) was added K2CO3 (4.85 g, 35.1 mmol). The reaction mixture was stirred at 70° C. for 4 h, then directly used into next step without workup and purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09051325B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-8562e7c7119a4ae18bd200313ce49d34 |
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| Source note | uspto-grants-2015_06 |
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