HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bicarbonate → HCID 59312926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bicarbonate | HCID 516893 | — |
| Reactant | 6-Chloro-3-nitropyridin-2-ylamine | HCID 2724035 | — |
| Reactant | tert-Butyl (2-aminopropyl)carbamate | HCID 22499135 | — |
| Product | HCID 59312926 | HCID 59312926 | — |
Reaction Steps
tert-Butyl {2-[(6-amino-5-nitropyridin-2-yl)amino]propyl}carbamate (Example 39A) is prepared in analogy to Example 38A from 2-amino-6-chloro-3-nitropyridine (637 mg, 3.7 mmol), tert-butyl (2-aminopropyl)carbamate (320 mg, 1.8 mmol) and potassium bicarbonate (368 mg, 3.7 mmol). 561 mg (98% of theory) of the product are obtained as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051323B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-5a42eff6c70b43818670f1ecabbb59ef |
| Source note | uspto-grants-2015_06 |