HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,5-DIMETHYL-5,6,7,8-TETRAHYDRONAPHTHALEN-2-OL → HCID 51029586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,5-DIMETHYL-5,6,7,8-TETRAHYDRONAPHTHALEN-2-OL | HCID 20287702 | — |
| Reactant | HCID 86668128 | HCID 86668128 | — |
| Product | HCID 51029586 | HCID 51029586 | 32% |
Reaction Steps
The title compound was prepared from toluene-4-sulfonic acid (S)-5-(1,1-difluoro-propyl)-7-oxo-2,3-dihydro-7H-oxazolo[3,2-a]pyrimidin-2-ylmethyl ester (0.188 mmol) and 5,5-dimethyl-5,6,7,8-tetrahydro-naphthalen-2-ol (0.281, mmol,) according to the procedure described in Example 9. This afforded 24.0 mg (32%) of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051331B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-b3376fa4d41441dd896bd52fc2c5e698 |
| Source note | uspto-grants-2015_06 |