HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 118023881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 118023509 | HCID 118023509 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 118023881 | HCID 118023881 | — |
Reaction Steps
To a mixture of 6-cyclohexyl-4-[(2,2-dimethylmorpholin-4-yl)methyl]-2-methylthieno[2,3-d]pyrimidine (130 mg) and EtOAc (2 mL) was added 4 M HCl/EtOAc (100 μL), followed by stirring at room temperature. The precipitated solid was collected by filtration to obtain 6-cyclohexyl-4-[(2,2-dimethylmorpholin-4-yl)methyl]-2-methylthieno[2,3-d]pyrimidine hydrochloride (90 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051339B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-1d3f4ff044174e59b7181d603b293be5 |
| Source note | uspto-grants-2015_06 |