HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 67303888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 70873584 | HCID 70873584 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67303888 | HCID 67303888 | 91% |
Reaction Steps
A 25% ammonia aqueous solution (20 ml) was added to (4-trifluoromethoxyphenoxy)acetic acid methyl ester in methanol (40 ml) and the mixture was stirred at room temperature overnight. After distilling the solvent off, the residue was washed with water and dried to afford the title compound as a white solid (12.1 g, yield 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051333B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-ad13d7e57a3e4972af851766e0ecca7f |
| Source note | uspto-grants-2015_06 |