HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12561346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Atropic acid | HCID 68114 | — |
| Reactant | tert-Butylcatechol | HCID 77643 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12561346 | HCID 12561346 | — |
Reaction Steps
and is prepared by treating a DMF solution of 2-phenyl-acrylic acid with thionyl chloride in the presence of tert-butylcatechol to afford 2-phenyl-acryloyl chloride. The latter is subsequently treated with a 30% aqueous solution of ammonia according to the following literature: K. Nishiyama, Y. Inouye Agric. Biol. Chem. 1982, 46, 1027-1034.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051448B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-3c925bd3b39b4b7a9116d6786224bbbe |
| Source note | uspto-grants-2015_06 |