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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2172407Generated: October 31, 2026

HCID 68006739, compound → HCID 86667391, compound

https://huagongshe.com/reaction/2172407

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68006739HCID 68006739—
ReactantHCID 86667392HCID 86667392—
ProductHCID 86667391HCID 8666739150.2%

Reaction Steps

8 g (0.024 mol) of 1,5,8,12,15,18,21-Heptaazacyclotricosane and 90.9 g (0.168 mol) of the trifluoromethyl oxonium salt were refluxed in an argon atmosphere for 3 hours to produce 9.7 g of 1,5,8,12,15,18,21-Heptakis(trifluoromethyl)-1,5,8,12,15,18,21-heptaazacyclotricosane represented by Formula 12 below.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09054392B2
Source datasetuspto-grants-2015_06
ORD IDord-c3056fc771f5470393dc391a0c4290c0
Source noteuspto-grants-2015_06