HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenethyl bromide → 1-[2-(4-Nitrophenyl)ethyl]-1,4-diazepane hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenethyl bromide | HCID 79266 | — |
| Reactant | Tert-butyl 1,4-diazepane-1-carboxylate | HCID 2756058 | — |
| Reactant | 1-[2-(4-Nitrophenyl)ethyl]piperazine hydrochloride | HCID 66644006 | — |
| Product | 1-[2-(4-Nitrophenyl)ethyl]-1,4-diazepane hydrochloride | HCID 67517347 | — |
Reaction Steps
1-[2-(4-nitrophenyl)ethyl]-1,4-diazepane hydrochloride was prepared in an analogous fashion to that described above for 1-[2-(4-nitrophenyl)ethyl]piperazine hydrochloride starting with 4-nitrophenethyl bromide and tert-butyl 1,4-diazepane-1-carboxylate. LC-MS: M+1=250.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-779644540e784c64aadd03ccc3e94a4f |
| Source note | uspto-grants-2015_06 |