HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-hydroxyethyl)-6-iodo-2-benzofuran-1(3H)-one → HCID 69087506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-hydroxyethyl)-6-iodo-2-benzofuran-1(3H)-one | HCID 66643870 | — |
| Reactant | HCID 67517481 | HCID 67517481 | — |
| Product | HCID 69087506 | HCID 69087506 | — |
Reaction Steps
tert-Butyl 4-[2-(6-iodo-1-oxo-1,3-dihydro-2-benzofuran-5-yl)ethyl]piperazine-1-carboxylate was prepared in an analogous fashion to that described for the preparation of tert-butyl 4-[2-(4-iodo-1-oxo-1,3-dihydro-2-benzofuran-5-yl)ethyl]piperazine-1-carboxylate above starting from 5-(2-hydroxyethyl)-6-iodo-2-benzofuran-1(3H)-one. LC-MS (IE, m/z): 473 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-dbbd2abcbd3b477b9bc0e3c96a0d59b2 |
| Source note | uspto-grants-2015_06 |