HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 89754304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 89754885 | HCID 89754885 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 89754304 | HCID 89754304 | — |
Reaction Steps
In a 12 mL reaction vial, was added tert-butyl 4-(2-[4-(methylsulfanyl)-1-oxo-1,3-dihydro-2-benzofuran-5-yl)ethyl]piperazine-1-carboxylate (25 mg, 0.064 mmol) and 4 N HCl in dioxane (1 mL). The reaction was stirred at r. t. for 18 hr. The reaction mixture was concentrated to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-32f3391552d14dd5ae08dd5efb975a12 |
| Source note | uspto-grants-2015_06 |