HuagongsheHuagongshe Chemistry Print Report · For research reference only
1374572-68-5 → HCID 86692997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1374572-68-5 | HCID 67515875 | — |
| Reactant | 4-methyl-5-(2-piperazin-1-ylethyl)-2-benzofuran-1(3H)-one hydrochloride | HCID 67517229 | — |
| Product | HCID 86692997 | HCID 86692997 | — |
Reaction Steps
5-[2-(piperazin-1-yl)ethyl]-6-(trifluoromethyl)-2-benzofuran-1(3H)-one hydrochloride was prepared in an analogous fashion to that described for the synthesis of 4-methyl-5-(2-piperazin-1-ylethyl)-2-benzofuran-1(3H)-one hydrochloride above starting from 5-bromo-6-(trifluoromethyl)-2-benzofuran-1(3H)-one. LC-MS (IE, m/z): 315 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-872e6ea70b45425490ce0d40eb2331d6 |
| Source note | uspto-grants-2015_06 |