HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67516969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 67517382 | HCID 67517382 | — |
| Product | HCID 67516969 | HCID 67516969 | — |
Reaction Steps
Compound tert-butyl 4-[(7-cyano-2,3-dihydro-1-benzofuran-3-yl)methyl]piperazine-1-carboxylate (76 mg, 0.22 mmol) was added HCl/dioxane (4 N) and the resulting mixture was stirred at room temperature for 3 hours, and then the solvents were removed under vacuum to give the crude 3-(piperazin-1-ylmethyl)-2,3-dihydro-1-benzofuran-7-carbonitrile hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-31ba23cfbbcc4fd59c18968fe233b6fc |
| Source note | uspto-grants-2015_06 |