HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 67517704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 67517556 | HCID 67517556 | — |
| Product | HCID 67517704 | HCID 67517704 | — |
Reaction Steps
A mixture of tert-butyl 4-{[5-(1H-tetrazol-1-yl)pyridin-2-yl]acetyl}piperazine-1-carboxylate (30 mg, 0.08 mmol) in HCl/EtOAc (5 mL) was stirred for 3 hours at room temperature. The reaction mixture was concentrated under reduce pressure to give 1-(piperazin-1-yl)-2-[5-(1H-tetrazol-1-yl)pyridin-2-yl]ethanone hydrochloride. MS m/z 274 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-7a1639d605e14dd88b3aa0b634c337c2 |
| Source note | uspto-grants-2015_06 |