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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2173363Generated: October 30, 2026

Acetic Acid → HCID 67515686, compound

https://huagongshe.com/reaction/2173363

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantHCID 77230645HCID 77230645—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67515686HCID 67515686—

Reaction Steps

A mixture of ethyl 2-(2-methyl-6-nitropyridin-3-yl)propanoate (1.6 g, 6.7 mmol), 10% Pd/C (0.1 g) and AcOH (3 mL) in MeOH (50 mL) was stirred over night under 1 atm of H2 at room temperature. The mixture was filtered and concentrated to give the crude product ethyl 2-(6-amino-2-methylpyridin-3-yl)propanoate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09056859B2
Source datasetuspto-grants-2015_06
ORD IDord-502f4218f66f4c7ba059ec69947359e5
Source noteuspto-grants-2015_06