HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Methoxy-4-nitrophenyl)acetic acid → HCID 18959618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Methoxy-4-nitrophenyl)acetic acid | HCID 16755859 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18959618 | HCID 18959618 | — |
Reaction Steps
A solution of (3-methoxy-4-nitrophenyl)acetic acid (2.08 g, 9.86 mmol) in 100 mL of EtOAc was added 600 mg of Pd/C under Ar, and the mixture was stirred at ambient temperature under H2 atmosphere overnight. The reaction mixture was filtered and the filtrate was concentrated to give (4-amino-3-methoxyphenyl)acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-ab1ad6dd398441939d861f6b455a6c3e |
| Source note | uspto-grants-2015_06 |